Journal1999
An Efficient Method for Production and Storage of Unstable S-Nitrosothiols Under Mild and Heterogeneous Condition with Sodium Nitrite and Oxalic Acid Dihydrate
Synthetic Communications Vol. 29, No. 13, 2277–2280
چکیده
Thiols can be readily converted to their corresponding nitrosothiols with a combination of oxalic acid and sodium nitrite in t-butanol at room temperature (26-30°C). The reaction mixture could be solidified with decreasing its temperature to, 15°C and was stored for several days without any destruction of the nitrosothiols.
موضوعات و کلیدواژهها
Chemical Synthesis and ReactionsSulfur-Based Synthesis TechniquesOrganic and Inorganic Chemical ReactionsChemistrySodium nitriteOxalic acidNitriteInorganic chemistrySodiumNuclear chemistryNitrateOrganic chemistry
ارجاع علمی
Mohammad Ali Zolfigol, Davood Nematollahi, Shadpour E Mallakpour. “An Efficient Method for Production and Storage of Unstable S-Nitrosothiols Under Mild and Heterogeneous Condition with Sodium Nitrite and Oxalic Acid Dihydrate.” Synthetic Communications, 1999. https://doi.org/10.1080/00397919908086229