Journal2012

Synthesis of Silica Bromide as Heterogeneous Reagent and its Application to Conversion of Alcohols to Alkyl Bromides

Farajollah Mohanazadeh, Mohammad Ali Zolfigol, Alireza Sedrpoushan, Hojat Veisi

Letters in Organic Chemistry Vol. 9, No. 8, 598–603

چکیده

Silica bromide as heterogeneous reagent is prepared from the reaction of silica gel with PBr3 as a nonhydroscopic, filterable, cheap, and stable yellowish powder that can be stored for months. The results show that the silica bromide is a suitable and efficient reagent for conversion of alcohols to alkyl bromides under mild conditions at room temperature. The easy availability of this reagent makes this simple procedure attractive and a practical alternative to the existing methods. Keywords: Alkyl bromides, bromination, heterogeneous reagent, silica bromide, polynucleotide, reactive substances, malodorous, polypeptide, intrapolymeric, phosphorus.

موضوعات و کلیدواژه‌ها

Chemical Synthesis and ReactionsReagentChemistryBromideAlkylHalogenationSilica gelOrganic chemistryCombinatorial chemistry

ارجاع علمی

Farajollah Mohanazadeh, Mohammad Ali Zolfigol, Alireza Sedrpoushan, Hojat Veisi. “Synthesis of Silica Bromide as Heterogeneous Reagent and its Application to Conversion of Alcohols to Alkyl Bromides.” Letters in Organic Chemistry, 2012. https://doi.org/10.2174/157017812802850285